;lgcp2d.mh ;Measure X-H dipolar coupling as the indirection dimension of a 2D ;magic-angle spin lock on 1H for CP without spin diffusion ;wr generally higher than 10 kHz ;Hong M, Yao XL, Jakes K, Huster D. ;J. Phys. Chem. B, volume 106, 7355, 2002 ;p3: 1H excitation pulse ;p21: 1H 55 deg. pulse ;p15: CP contact time ;p8: 1H TPPM dec. pulse ;pl2: 1H excitation power ;pl3: 1H LG-CP power ;pl1: 13C CP power, w1H,eff (+/-) wr ;FQ2: LG-CP ;FQ3: on resonance ;d1: recycle delay ;l31: spinning speed in Hz "p21=p3*353/900" "l1=aq/(p8*2)" "d3=1s/l31" 1 ze 2 d1 10u pl1:f1 10u pl2:f2 2u:f2 ph1 2u:f1 ph2 3 p3:f2 ph1 ;90 deg pulse p21:f2 ph3 ;35 deg pulse 0.5u fq2:f2 ;put 1H off resonance 0.5u pl3:f2 (p15 ph2):f1 (p15 ph10):f2 ;CP, t1 1u fq3:f2 ;put 1H back on res for decoupling 1u cw:f2 pl12:f2 ;pl11:f1 1u:f1 ph0 ;dead time delay, reset RF phase to detect 2u adc ph31 ;start ADC with ph31 signal routing 6 p8:f2 ph13 ;TPPM decoupling p8:f2 ph14 lo to 6 times l1 aq do:f2 d3 rcyc=2 ; wr #0 ;2D ;States' detection 200m wr #0 if #0 zd ;write file to disk, increment, zero data 10m ipu15 lo to 1 times td1 exit ph0= +x ph1= -y +y ;1H excitation ph3= +y ;35 deg pulse ph10= +x ;1H LG-CP ph2= +x +x +y +y -x -x -y -y ;X CP spin lock ph4= -x -x -y -y +x +x +y +y ph13=(360) 0 ph14=(360) 10 ph31= 2 0 3 1 0 2 1 3